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QA/QC measures undertaken to ensure high integrity data

  1. NUERS' analytical procedures following the SOPs based on international methods, satisfying the defined QC criteria to produce accurate and reliable results.

  2. All the instruments are calibrated at the beginning of each batch of analysis using the chemical standards as per SOPs. Routine annual maintenance schedules are in place for all major instruments, and monitoring systems like thermometers, balances etc.

  3. NUERS utilizes a variety of in-house analytical methods that are based on the most recent versions of internationally recognized methods. In some cases, minor modifications of the reference methodology such modifications are listed in the corresponding SOPs may be employed. Accuracy, precision and sensitivity must be within the acceptance criteria of the reference methods.

  4. NUERS adopts the QC protocol of international standard methods (USEPA, MOOPAM, ASTM) as described in Quality Assurance Manual (QAM), and consistent with NUERS’ objectives, policies, facilities, organization, personnel, services, and specific QA and quality control (QC) procedures as practiced within each area of operation. The content of the QAM sections is not modified for specific customers or agencies, unless the requirements of these customers constitute their standard policy. Customer-specific requirements are included in COC, or in the customer-specific sections of the operational SOPs, as appropriate.

  • Organic Analysis
  • Organic Extraction Analysis
  • Inorganic Analysis
  • Soil Lab

Organic Analysis

Test Name

Matrix

Aliphatic Hydrocarbon Profile By GC/FID-(C8-C40)Soil, Water, Filter, Fish tissue (Biota)
Total Petroleum Hydrocarbons By GC/FID-(C8-C40)Water, Soil, Air Filter
Polycyclic Aromatic Hydrocarbons - 16 Priority Pollutant Compounds by GC/MSWater, Soil, Air Filter, Fish Tissue (Biota)
Organochlorine Pesticides By GC/MSWater, Soil, Fish Tissue (Biota)
GC-FID AnalysisChemicals, Oil
GC-MS AnalysisChemicals, Oil
UPLC-PDA AnalysisExtracts of Food, Water, chemicals

Organic Extraction Analysis

Test Name

Matrix

TPH as Hexane Extractable Material (HEM) by Gravimetry Soil/Water
Oil & Grease by GravimetryWater/Plastic
TPH as Extractable Organic Material (EOM) by GravimetrySoil
Lipid Content by GravimetryBiota
Separatory Funnel ExtractionsWater
Extraction by Microwave Assisted Extractor (MAE)Soil/ Biota/ Vegetation
Simple Distillation by Parallel EvaporatorLiquids
Total Organic Matter (TOM) by GravimetrySoil / Vegetation
Extraction by Accelerated Solvent Extractor/ Pressurized Solvent ExtractorSoil/Biota/Food/Vegetation
Extraction by Ultrasonic ExtractorAir filter
Solvent Recovery by Parallel EvaporatorLiquids
Determination of Crude & Total fat and unsaponified & saponified fat by Automated Solvent ExtractorFood/Biota/Soil/Vegetation
Determination of unsaponified & saponified fatSolid
Saponification ValueOil / Fat
Un saponification ValueOil / Fat

Inorganic Analysis

Test Name

Matrix

Acid Digestion for Metals AnalysisSoil, Water, Air filter, Fish tissue (Biota), Oil
Mercury Analysis by Hg AnalyzerSoil, Water, Air filter, Fish tissue (Biota)
Acid Digestion for Mercury AnalysisSoil, Water, Air filter, Fish tissue (Biota), Solid
Specific Conductance by Ion Selective ElectrodeSoil / Water
pH Analysis by Ion Selective ElectrodeSoil / Water
Turbidity (Nephelometric)Water
Alkalinity by titrationSoil, Water
Salinity by Argentometric Method by titrationSoil, Water
Ammonia by Lachat FIA (Flow Injection AnalyzerSoil/Water
Ortho-Phosphate by Lachat FIASoil/Water
Total Phosphorus by Lachat FIASoil/Water
Silicate by Lachat FIASoil/Water
Total Organic CarbonSoil/Water/Sludge
Total CarbonSoil/Water/Sludge
Anion Analysis by IC (F-, Cl-, Br-, SO4-,   NO3-, ClO3- )Water
Ash ContentSolid / Vegetation
COD by Nanocolor VIS II SpectrophotometerWater/Soil
Total HardnessWater
TSS by TSS MeterWater
BODWater
Temperature detectionWater
AciditySoil/Water
SAR - Sodium Absorption RatioSoil/Water
Dissolved OxygenWater
Boron by Discrete analyzerSoil and Water
Sulfide by Discrete analyzerSoil and Water
TOM (Total Organic Matter)Soil
Metal Analysis by ICP OESSoil, Water, Air filter, Fish tissue (Biota), Oil

Soil Lab

Test Name

Matrix

Gross Calorific Value by Bomb CalorimeterCoal/ Coke
Gross Calorific and Ash Value by Bomb CalorimeterWaste material
Gross Calorific Value of Refuse-Derived Fuel by the Bomb Calorimeter”Solid fuel
Carbon, Hydrogen, Nitrogen analysis in Sediment, plant, coal and coke by Elemental AnalyzerSediment, Coal and coke
Sulfur analysis in Sediment, plant, Coal, coke and ash by Elemental AnalyzerSediment, Coal, coke and ash
Particle Size Analysis of Soil Samples by GravimetrySoil
Total Dissolved Solids (TDS) by GravimetryWater
Total Suspended Solids, Non-filterable Residue (TSS) by GravimetryWater
Percent moisture by GravimetrySoil
Percent moisture by Freeze dryerWater, Soil, Fish tissue (Biota), Vegetation