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QA/QC measures undertaken to ensure high integrity data

  1. NUERS' analytical procedures following the SOPs based on international methods, satisfying the defined QC criteria to produce accurate and reliable results.

  2. All the instruments are calibrated at the beginning of each batch of analysis using the chemical standards as per SOPs. Routine annual maintenance schedules are in place for all major instruments, and monitoring systems like thermometers, balances etc.

  3. NUERS utilizes a variety of in-house analytical methods that are based on the most recent versions of internationally recognized methods. In some cases, minor modifications of the reference methodology such modifications are listed in the corresponding SOPs may be employed. Accuracy, precision and sensitivity must be within the acceptance criteria of the reference methods.

  4. NUERS adopts the QC protocol of international standard methods (USEPA, MOOPAM, ASTM) as described in Quality Assurance Manual (QAM), and consistent with NUERS’ objectives, policies, facilities, organization, personnel, services, and specific QA and quality control (QC) procedures as practiced within each area of operation. The content of the QAM sections is not modified for specific customers or agencies, unless the requirements of these customers constitute their standard policy. Customer-specific requirements are included in COC, or in the customer-specific sections of the operational SOPs, as appropriate.

  • Organic Analysis
  • Organic Extraction Analysis
  • Inorganic Analysis
  • Soil Lab

Organic Analysis

Test Name

Matrix

Aliphatic Hydrocarbon Profile By GC/FID-(C8-C40) Soil, Water, Filter, Fish tissue (Biota)
Total Petroleum Hydrocarbons By GC/FID-(C8-C40) Water, Soil, Air Filter
Polycyclic Aromatic Hydrocarbons - 16 Priority Pollutant Compounds by GC/MS Water, Soil, Air Filter, Fish Tissue (Biota)
Organochlorine Pesticides By GC/MS Water, Soil, Fish Tissue (Biota)
GC-FID Analysis Chemicals, Oil
GC-MS Analysis Chemicals, Oil
UPLC-PDA Analysis Extracts of Food, Water, chemicals

Organic Extraction Analysis

Test Name

Matrix

TPH as Hexane Extractable Material (HEM) by Gravimetry  Soil
TPH as Hexane Extractable Material (HEM) by Gravimetry Water
Oil & Grease by Gravimetry Water/Plastic
TPH as Extractable Organic Material (EOM) by Gravimetry Soil
Lipid Content by Gravimetry Biota
Determination of PHCs by UVF Soil/Water/ Fish Tissue(Biota)
Soxhlet, and Separatory Funnel Extractions Soil/Water/Biota/ Vegetation
Extraction by Microwave Assisted Extractor (MAE) Soil/ Biota/ Vegetation
Simple Distillation Liquids / Salts
Simple Distillation by Parallel Evaporator Liquids / Salts
Total Organic Matter (TOM) by Gravimetry Soil / Vegetation
Extraction by Accelerated Solvent Extractor/ Pressurized Solvent Extractor Soil/Water/Biota/Food/Vegetation
Extraction by Ultrasonic Extractor Air filter
Extraction by Automated Solvent Extractor Soil/Water/Biota/Food/Vegetation
Solvent Recovery by Parallel Evaporator Liquids
Determination of Crude & Total fat Food
Determination of unsaponified & saponified fat Solid
Saponification Value Oil / Fat
Un saponification Value Oil / Fat

Inorganic Analysis

Test Name

Matrix

Acid Digestion for Metals Analysis Soil, Water, Air filter, Fish tissue (Biota), Oil
Mercury Analysis by Hg Analyzer Soil, Water, Air filter, Fish tissue (Biota)
Acid Digestion for Mercury Analysis Soil, Water, Air filter, Fish tissue (Biota), Solid
Specific Conductance by Ion Selective Electrode Soil / Water
pH Analysis by Ion Selective Electrode Soil / Water
Turbidity (Nephelometric) Water
Alkalinity by titration Soil, Water
Salinity by Argentometric Method by titration Soil, Water
Ammonia by Lachat FIA (Flow Injection Analyzer Soil/Water
Ortho-Phosphate by Lachat FIA Soil/Water
Total Phosphorus by Lachat FIA Soil/Water
Silicate by Lachat FIA Soil/Water
Total Organic Carbon Soil/Water/Sludge
Total Nitrogen Soil/Water/Sludge
Total Carbon Soil/Water/Sludge
Anion Analysis by IC (F-, Cl-, Br-, SO4-,   NO3-, ClO3- ) Water
Ash Content Solid / Vegetation
COD by Nanocolor VIS II Spectrophotometer Water/Soil
UV-General Scan Liquid
Total Hardness Water
TSS by TSS Meter Water
BOD Water
Temperature detection Water
Acidity Soil/Water
SAR - Sodium Absorption Ratio Soil/Water

Soil Lab

Test Name

Matrix

Gross Calorific Value by Bomb Calorimeter Coal/ Coke
Gross Calorific and Ash Value by Bomb Calorimeter Waste material
Gross Calorific Value of Refuse-Derived Fuel by the Bomb Calorimeter” Solid fuel
Carbon, Hydrogen, Nitrogen analysis in Sediment, plant, coal and coke by Elemental Analyzer Sediment, Coal and coke
Sulfur analysis in Sediment, plant, Coal, coke and ash by Elemental Analyzer Sediment, Coal, coke and ash
Particle Size Analysis of Soil Samples by Gravimetry Soil
Total Dissolved Solids (TDS) by Gravimetry Water
Total Suspended Solids, Non-filterable Residue (TSS) by Gravimetry Water
Percent moisture by Gravimetry Soil
Percent moisture by Freeze dryer Water, Soil, Fish tissue (Biota), Vegetation
Bulk Density by Gravimetry Soil
Specific Gravity Soil